{Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}

Base Information

Chemical Name:{Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}
CAS No.:110981-75-4
Molecular Formula:C₂₆H₂₁N₂O₂PRu
Molecular Weight:525.509
Hs Code.:

{Ru(C<sub>6</sub>H<sub>4</sub>(NH)2)(CO)2(P(C<sub>6</sub>H<sub>5</sub>)3)}

Synonyms:{Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}

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Chemical Property of {Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}

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Technology Process of {Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}

There total 3 articles about {Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 72557-06-3
{Ru(μ-1,2-(NH)2C6H4)(P(C6H5)3)3}

: 20332-49-4,14741-36-7
tricarbonylbis(triphenylphosphine)ruthenium⁽⁰⁾

: [μ,μ'-1,2-phenylenediimine-(N,N')-dicarbonylbis(triphenylphosphine)diruthenium(Ru-Ru)]

: 72557-05-2
{Ru(C₆H₄(NH)2)(CO)(P(C₆H₅)3)2}

: 110981-75-4
{Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}

Guidance literature:: With CO; In toluene; CO is bubbled through the solution at room temp. for 4 h; the main product Ru(1,2-C6H4(NH)2)(CO)(PPh3)2 is obtained on addition of light petroleum; when the reaction soln. is chromd. on Al2O3 (eluate:toluene), further Ru complexes can be isolated; recrystn. of dinuclear Rucomplex from light petroleum/toluene;
DOI:10.1016/0022-328X(87)80217-6

Reference yield:

: 72557-05-2
{Ru(C₆H₄(NH)2)(CO)(P(C₆H₅)3)2}

: 110981-75-4
{Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}

Guidance literature:: With CO; In toluene; CO was bubbled through a soln. of (Ru(C6H4(NH)2)(CO)(PPh3)2) in toluene at room temp. for 3 h; addn. of hexane; the filtered soln. was left at -20°C for 5 h; performed under N2 using Schlenk technique;; the ppt. was filtered off, washed with hexane, and dried under vac.; elem. anal.;;
DOI:10.1039/DT9930001125

Reference yield:

: 72557-06-3
{Ru(C₆H₄(NH)2)(P(C₆H₅)3)3}

: 72557-05-2
{Ru(C₆H₄(NH)2)(CO)(P(C₆H₅)3)2}

: 110981-75-4
{Ru(C₆H₄(NH)2)(CO)2(P(C₆H₅)3)}

Guidance literature:: With CO; In toluene; CO was bubbled through a soln. of (Ru(C6H4(NH)2)(PPh3)3) in toluene at room temp. for 3 h; addn. of hexane; the filtered soln. was left at -20°C for 5 h; performed under N2 using Schlenk technique;; the ppt. was filtered off, washed with hexane, and dried under vac.; mixt. obtained, detected by IR spectroscopy;;
DOI:10.1039/DT9930001125