6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine

Base Information

Chemical Name:6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine
CAS No.:1407829-49-5
Molecular Formula:C₁₇H₁₅ClN₄
Molecular Weight:310.786
Hs Code.:

Synonyms:6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine

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Chemical Property of 6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine

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Technology Process of 6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine

There total 7 articles about 6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 1407832-63-6
6-(4-chlorophenyl)-1-methyl-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepin-5(6H)-one

: 1407829-49-5
6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine

Guidance literature:: With borane-THF; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 106-47-8
4-chloro-aniline

: 1407829-49-5
6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; potassium fluoride / dichloromethane / 0.47 h / 220 °C / Microwave irradiation

2: ammonium chloride; iron / ethanol; water / 2 h / 70 °C

3: toluene / Reflux

4: tetraphosphorus decasulfide / pyridine / 1 h / Reflux; Inert atmosphere

5: butan-1-ol / 24 h / Reflux; Inert atmosphere

6: borane-THF / tetrahydrofuran / 2 h / 20 °C

With potassium fluoride; tetraphosphorus decasulfide; borane-THF; iron; potassium carbonate; ammonium chloride; In tetrahydrofuran; pyridine; ethanol; dichloromethane; water; toluene; butan-1-ol;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1407829-49-5
6-(4-chlorophenyl)-1-methyl-5,6-dihydro-4H-benzo[b][1,2,4]triazolo[4,3-d][1,4]diazepine

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; potassium fluoride / dichloromethane / 0.47 h / 220 °C / Microwave irradiation

2: ammonium chloride; iron / ethanol; water / 2 h / 70 °C

3: toluene / Reflux

4: tetraphosphorus decasulfide / pyridine / 1 h / Reflux; Inert atmosphere

5: butan-1-ol / 24 h / Reflux; Inert atmosphere

6: borane-THF / tetrahydrofuran / 2 h / 20 °C

With potassium fluoride; tetraphosphorus decasulfide; borane-THF; iron; potassium carbonate; ammonium chloride; In tetrahydrofuran; pyridine; ethanol; dichloromethane; water; toluene; butan-1-ol;