4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde

Base Information

Chemical Name:4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde
CAS No.:866768-45-8
Molecular Formula:C₄₉H₄₈O₃S₄
Molecular Weight:813.182
Hs Code.:

Synonyms:4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde

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Chemical Property of 4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde

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Technology Process of 4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde

There total 4 articles about 4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₃H₅₈O₄S₄

: 866768-45-8
4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde

Guidance literature:: With hydrogenchloride; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/chem.200500073

Reference yield:

: 2,5-bis(dimethylphosphonatomethyl)-1,4-dihexyloxybenzene

: 866768-45-8
4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-BuOK / tetrahydrofuran / 0.33 h

1.2: 41 percent / tetrahydrofuran / 2 h

2.1: t-BuOK / tetrahydrofuran / 16 h / 20 °C

3.1: 115 mg / aq. HCl / CH₂Cl₂ / 16 h / 20 °C

With hydrogenchloride; potassium tert-butylate; In tetrahydrofuran; dichloromethane; 1.2: Wittig-Horner olefination / 2.1: Wittig-Horner reaction;
DOI:10.1002/chem.200500073

Reference yield:

: 866768-38-9
{4-[(E)-2-(4-Diethoxymethyl-phenyl)-vinyl]-2,5-bis-hexyloxy-benzyl}-phosphonic acid dimethyl ester

: 866768-45-8
4-((E)-2-{4-[(E)-2-(9,10-Bis-[1,3]dithiol-2-ylidene-9,10-dihydro-anthracen-2-yl)-vinyl]-2,5-bis-hexyloxy-phenyl}-vinyl)-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / tetrahydrofuran / 16 h / 20 °C

2: 115 mg / aq. HCl / CH₂Cl₂ / 16 h / 20 °C

With hydrogenchloride; potassium tert-butylate; In tetrahydrofuran; dichloromethane; 1: Wittig-Horner reaction;
DOI:10.1002/chem.200500073