N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide

Base Information

Chemical Name:N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide
CAS No.:1282613-24-4
Molecular Formula:C₂₂H₂₂ClN₃O₂S
Molecular Weight:427.955
Hs Code.:

Synonyms:N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide

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Chemical Property of N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide

Chemical Property:

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Technology Process of N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide

There total 6 articles about N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1220870-13-2
5-[4-(allyloxy)-3,5-dimethylphenyl]-N-butyl-1,3,4-thiadiazol-2-amine

: 609-65-4
o-chlorobenzoyl chloride

: 1282613-24-4
N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide

Guidance literature:: 5-[4-(allyloxy)-3,5-dimethylphenyl]-N-butyl-1,3,4-thiadiazol-2-amine; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

o-chlorobenzoyl chloride; In tetrahydrofuran; at 20 ℃; for 1.5h;

Reference yield:

: 592-82-5
butyl isothiocyanate

: 1282613-24-4
N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / methanol / 10 - 15 °C

2.1: trichlorophosphate / 1,4-dioxane / 20 - 80 °C

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3.2: 1.5 h / 20 °C

With sodium hydride; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol;

Reference yield:

: 100191-87-5
4-(allyloxy)-3,5-dimethylbenzonitrile

: 1282613-24-4
N-(5-(4-(allyloxy)phenyl)-1,3,4-thiadiazol-2-yl)-N-butyl-2-chlorobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; water / ethanol / 20 - 110 °C / Sealed

1.2: pH 1

2.1: trichlorophosphate / 1,4-dioxane / 20 - 80 °C

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3.2: 1.5 h / 20 °C

With water; sodium hydride; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol;