N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide

Base Information

Chemical Name:N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide
CAS No.:1310048-46-4
Molecular Formula:C₂₂H₂₃N₅O₄
Molecular Weight:421.456
Hs Code.:

Synonyms:N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide

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Technology Process of N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide

There total 2 articles about N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1310048-45-3
6-amino-N-(3-azidopropyl)-2-naphthamide

: 95298-68-3
3-methoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid

: 1310048-46-4
N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 120 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1002/anie.201007871

Reference yield:

: 116668-47-4
6-amino-2-naphthoic acid

: 1310048-46-4
N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1002/anie.201007871

Reference yield: 92.0%

: 1310048-46-4
N-(3-azidopropyl)-6-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-2-naphthamide

: 1310048-36-2
C₂₁H₂₁N₅O₄

Guidance literature:: With ammonium cerium (IV) nitrate; water; In acetonitrile; at 95 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201007871