3-chlorobenzophenone 4-methylphenylsulfonylhydrazone

Base Information

• Chemical Name: 3-chlorobenzophenone 4-methylphenylsulfonylhydrazone
• CAS No.: 119870-88-1
• Molecular Formula: C₂₀H₁₇ClN₂O₂S
• Molecular Weight: 384.886
• Mol file: 119870-88-1.mol

Synonyms:3-chlorobenzophenone 4-methylphenylsulfonylhydrazone

Chemical Property of 3-chlorobenzophenone 4-methylphenylsulfonylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-chlorobenzophenone 4-methylphenylsulfonylhydrazone

There total 1 articles about 3-chlorobenzophenone 4-methylphenylsulfonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

3-chlorobenzophenone (1016-78-0) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 3-chlorobenzophenone 4-methylphenylsulfonylhydrazone (119870-88-1)

Guidance literature:

With acetyl chloride; In ethanol; for 10.5h; Heating;

DOI:10.1021/ol0711117

Reference yield: 65.0%

3-chlorobenzophenone 4-methylphenylsulfonylhydrazone (119870-88-1) → 3-(3-chlorophenyl)-1-(4-methylphenylsulfonyl)indazole + 5-Chlor-3-phenyl-1-(4-methylbenzolsulfonyl)-1H-indazol (102276-46-0)

Guidance literature:

With copper diacetate; silver trifluoroacetate; palladium diacetate; In dimethyl sulfoxide; at 50 ℃; for 20h;

DOI:10.1021/ol0711117

Reference yield: 63.0%

3-chlorobenzophenone 4-methylphenylsulfonylhydrazone (119870-88-1) → 3-chloro-N-phenylbenzamide (6832-92-4)

Guidance literature:

upstream raw materials:

3-chlorobenzophenone

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

3-chloro-N-phenylbenzamide

5-Chlor-3-phenyl-1-(4-methylbenzolsulfonyl)-1H-indazol