2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine

Base Information

Chemical Name:2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine
CAS No.:915107-04-9
Molecular Formula:C₃₈H₄₀N₄O₃
Molecular Weight:600.761
Hs Code.:

Synonyms:2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine

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Chemical Property of 2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine

Chemical Property:

Purity/Quality:

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Technology Process of 2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine

There total 1 articles about 2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Indole-2-carboxylic acid: 1477-50-5,1228050-17-6
Indole-2-carboxylic acid

: 253873-18-6
3-(N,N-diethylaminocarbonyloxymethyl)-1-(triphenylmethyl)piperazine

: 915107-04-9
2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine

Guidance literature:: With diisopropyl-carbodiimide; In dichloromethane; Heating;
DOI:10.1016/j.bmc.2006.07.043

Reference yield:

: 915107-04-9
2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine

: diethyl-carbamic acid 4-benzyl-1-(1H-indole-2-carbonyl)-piperazin-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / trifluoroacetic acid / methanol / 0.33 h / 20 °C

2: 93 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 20 °C

With sodium tris(acetoxy)borohydride; trifluoroacetic acid; In methanol; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2006.07.043

Reference yield:

: 915107-04-9
2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(triphenylmethyl)piperazine

: 2-(N,N-diethylaminocarbonyloxymethyl)-1-(1H-indole-2-carbonyl)-4-(3,4,5-trimethoxybenzyl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / trifluoroacetic acid / methanol / 0.33 h / 20 °C

2: 95 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 20 °C

With sodium tris(acetoxy)borohydride; trifluoroacetic acid; In methanol; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2006.07.043