NH2-PheΨAib-Phe-OEt

Base Information

Chemical Name:NH2-PheΨAib-Phe-OEt
CAS No.:227612-10-4
Molecular Formula:C₂₁H₃₃N₃O₃S
Molecular Weight:407.577
Hs Code.:

Synonyms:NH2-PheΨAib-Phe-OEt

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Chemical Property of NH2-PheΨAib-Phe-OEt

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Technology Process of NH2-PheΨAib-Phe-OEt

There total 3 articles about NH2-PheΨAib-Phe-OEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 227612-00-2
FMOC-IleΨAib-Phe-OEt

: 227612-10-4
NH2-PheΨAib-Phe-OEt

Guidance literature:: With diethylamine; In acetonitrile; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(99)00234-3

Reference yield:

: 227611-94-1
[(1S,2S)-1-(4,4-Dimethyl-5-oxo-4,5-dihydro-thiazol-2-yl)-2-methyl-butyl]-carbamic acid 9H-fluoren-9-ylmethyl ester

: 227612-10-4
NH2-PheΨAib-Phe-OEt

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / DIEA, HOBt / acetonitrile / 336 h / Ambient temperature

2: Et₂NH / acetonitrile / 1 h / Ambient temperature

With benzotriazol-1-ol; diethylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1016/S0040-4020(99)00234-3

Reference yield:

: 227612-07-9
(9H-Fluoren-9-yl)methyl N-<(1S,2S)-2-methyl-1-<<<1,1-dimethyl-2--2-oxoethyl>amino>thioxomethyl>butyl>carbamate

: 227612-10-4
NH2-PheΨAib-Phe-OEt

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / (+/-)-camphor-10-sulfonic acid / CH₂Cl₂ / 0.03 h / Ambient temperature

2: 55 percent / DIEA, HOBt / acetonitrile / 336 h / Ambient temperature

3: Et₂NH / acetonitrile / 1 h / Ambient temperature

With camphor-10-sulfonic acid; benzotriazol-1-ol; diethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(99)00234-3