C₃₅H₃₉I₂NO₂

Base Information

Chemical Name:C₃₅H₃₉I₂NO₂
CAS No.:1347067-83-7
Molecular Formula:C₃₅H₃₉I₂NO₂
Molecular Weight:759.509
Hs Code.:

C<sub>35</sub>H<sub>39</sub>I<sub>2</sub>NO<sub>2</sub>

Synonyms:C₃₅H₃₉I₂NO₂

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Chemical Property of C₃₅H₃₉I₂NO₂

Chemical Property:

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Technology Process of C₃₅H₃₉I₂NO₂

There total 1 articles about C₃₅H₃₉I₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75867-46-8
2,6-diethynylpyridine

: 314250-11-8
1-hexyloxymethyl-3,5-diiodbenzene

: 1347067-83-7
C₃₅H₃₉I₂NO₂

Guidance literature:: 2,6-diethynylpyridine; 1-hexyloxymethyl-3,5-diiodbenzene; With triethylamine; In toluene; at 20 ℃; for 0.5h; Inert atmosphere;

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo2018944

Reference yield: 90.0%

: 1347067-83-7
C₃₅H₃₉I₂NO₂

: 1066-54-2
trimethylsilylacetylene

: 1347067-85-9
C₄₅H₅₇NO₂Si₂

Guidance literature:: C₃₅H₃₉I₂NO₂; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

trimethylsilylacetylene; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo2018944

Reference yield:

: 1347067-83-7
C₃₅H₃₉I₂NO₂

: 1347067-88-2
C₃₉H₄₁NO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: methanol; potassium carbonate / dichloromethane / 20 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; 1.2: Sonogashira cross-coupling;
DOI:10.1021/jo2018944