o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-L-threoninate

Base Information

Chemical Name:o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-L-threoninate
CAS No.:86117-93-3
Molecular Formula:C₅₂H₅₂N₂O₁₂
Molecular Weight:896.991
Hs Code.:

Synonyms:o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-L-threoninate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-L-threoninate

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Technology Process of o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-L-threoninate

There total 3 articles about o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-L-threoninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 62087-89-2
ester O-nitrophenylique de la N-(benzyloxycarbonyl)-L-threonine

: 77871-01-3,77943-03-4,86117-93-3,86161-21-9
ester-O-nitrophenolique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-L-threonine

: 77871-01-3,77943-03-4,86117-93-3,86161-21-9
ester-O-nitrophenolique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine

Guidance literature:: With trifluoromethanesulfonic acid anhydride; In dichloromethane; acetonitrile; at -20 ℃; for 0.5h;

Reference yield: 40.0%

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 62087-89-2
ester O-nitrophenylique de la N-(benzyloxycarbonyl)-L-threonine

: 77871-01-3,77943-03-4,86117-93-3,86161-21-9
ester-O-nitrophenolique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-L-threonine

: 77871-01-3,77943-03-4,86117-93-3,86161-21-9
ester-O-nitrophenolique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine

Guidance literature:: With trifluoromethanesulfonic acid anhydride; In dichloromethane; acetonitrile; at -20 ℃; for 0.5h;

Reference yield: 37.0%

: 6386-24-9
2,3,4,6-tetra-O-benzyl-D-galactopyranose

: 62087-89-2
ester O-nitrophenylique de la N-(benzyloxycarbonyl)-L-threonine

: 86117-93-3
o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-L-threoninate

: 86161-21-9
o-nitrophenyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-L-threoninate

Guidance literature:: With trifluoromethanesulfonic acid anhydride; In dichloromethane; acetonitrile; at -15 ℃; for 0.25h;
DOI:10.1021/jo00163a027