Technology Process of C25H32O3S2
There total 1 articles about C25H32O3S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-Bromosuccinimide / tetrahydrofuran / 15 h / 25 °C
2.1: magnesium / tetrahydrofuran / 0.5 h / Reflux
2.2: 15 h / Reflux
3.1: boron tribromide / dichloromethane / 24 h / -78 - 25 °C
4.1: potassium carbonate / acetonitrile / 6 h / Reflux
5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 25 °C
With
N-Bromosuccinimide; osmium(VIII) oxide; boron tribromide; potassium carbonate; magnesium; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; water; acetone; acetonitrile;
2.2: |Kumada Cross-Coupling;
DOI:10.1039/c3sc50664a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / 24 h / 25 °C
2: n-butyllithium; copper dichloride / tetrahydrofuran / 15 h / -60 °C / Reflux
3: hydrogenchloride / water; methanol / 24 h / 25 °C
With
hydrogenchloride; n-butyllithium; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; copper dichloride;
In
tetrahydrofuran; methanol; water;
DOI:10.1039/c3sc50664a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / 24 h / 25 °C
2: n-butyllithium; copper dichloride / tetrahydrofuran / 15 h / -60 °C / Reflux
With
n-butyllithium; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; copper dichloride;
In
tetrahydrofuran;
DOI:10.1039/c3sc50664a
