Technology Process of C28H32O7S
There total 12 articles about C28H32O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
DOI:10.1021/ol102390t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 12 h / 20 °C
2: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C
With
sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1021/ol102390t
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / 1.83 h / -40 - 20 °C / Inert atmosphere
2: di(n-butyl)tin oxide; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere
3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 12 h / 20 °C
4: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C
With
sodium periodate; osmium(VIII) oxide; di(n-butyl)tin oxide; 4-methylmorpholine N-oxide; triethylamine;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol102390t