2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on

Base Information

• Chemical Name: 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on
• CAS No.: 103929-40-4
• Molecular Formula: C₂₀H₂₂Cl₂N₆O₂
• Molecular Weight: 449.34

Synonyms:2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on

Chemical Property of 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on

Chemical Property:

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Technology Process of 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on

There total 3 articles about 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C20H22Cl2N6O2 (103929-42-6) → 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on (103929-40-4)

Guidance literature:

With silica gel; In diethyl ether; Petroleum ether; for 4h;

DOI:10.1007/BF00809197

Reference yield: 22.0%

1-(4-Chlorphenylazo)-1-methylethylisocyanat (28359-16-2) → 2-(4-Chlorphenyl)-5,5-dimethyl-1,2,4-triazolidin-3-on (72731-37-4) + 2-(4-Chlorphenyl)-1-ethyl-5,5-dimethyl-1,2,4-triazolidin-3-on (103945-79-5) + 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on (103929-40-4) + 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-1-ethyl-5,5-dimethyl-1,2,4-triazolidin-3-on (103929-39-1)

Guidance literature:

With ethylmagnesium bromide; In diethyl ether; at 0 - 5 ℃; for 3h; Further byproducts given;

DOI:10.1007/BF00809197

Reference yield:

1-(4-Chlorphenylazo)-1-methylethylisocyanat (28359-16-2) + 2-(4-Chlorphenyl)-5,5-dimethyl-1,2,4-triazolidin-3-on (72731-37-4) → C20H22Cl2N6O2 (103929-42-6) + 2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonyl-5,5-dimethyl-1,2,4-triazolidin-3-on (103929-40-4)

Guidance literature:

With ethylmagnesium bromide; Yield given. Multistep reaction; 1.) ether, 10 min; 2.) ether, 5 h;

DOI:10.1007/BF00809197

upstream raw materials:

1-(4-Chlorphenylazo)-1-methylethylisocyanat

2-(4-Chlorphenyl)-5,5-dimethyl-1,2,4-triazolidin-3-on

C₂₀H₂₂Cl₂N₆O₂

Downstream raw materials:

C₂₀H₂₂Cl₂N₆O₂

2-(4-Chlorphenyl)-4-<1-(4-chlorphenylazo)-1-methylethyl>-aminocarbonylsemicarbazid

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