(2-fluorophenyl)octylamine

Base Information

Chemical Name:(2-fluorophenyl)octylamine
CAS No.:936747-22-7
Molecular Formula:C₁₄H₂₂FN
Molecular Weight:223.334
Hs Code.:

Synonyms:(2-fluorophenyl)octylamine

Suppliers and Price of (2-fluorophenyl)octylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-fluorophenyl)octylamine

Chemical Property:

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Technology Process of (2-fluorophenyl)octylamine

There total 3 articles about (2-fluorophenyl)octylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 348-54-9
2-Fluoroaniline

: 111-83-1
1-bromo-octane

: 936747-22-7
(2-fluorophenyl)octylamine

Guidance literature:: With sodium dodecyl-sulfate; sodium hydrogencarbonate; In water; at 80 ℃; for 12h;
DOI:10.1002/ejoc.200600937

Reference yield: 69.0%

: 348-54-9
2-Fluoroaniline

: 538-23-8
tricaprilin

: 936747-22-7
(2-fluorophenyl)octylamine

Guidance literature:: With tris(2,4-pentanedionato)ruthenium(III); hydrogen; bis(trifluoromethanesulfonyl)amide; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; In tetrahydrofuran; at 150 ℃; for 18h; under 45004.5 Torr; Autoclave;
DOI:10.1002/anie.201603681

Reference yield:

: 348-54-9
2-Fluoroaniline

: 629-05-0
n-octyne

: 936747-22-7
(2-fluorophenyl)octylamine

: C₁₄H₂₂FN

Guidance literature:: 2-Fluoroaniline; n-octyne; With Ti(3-(1H-pyrrol-2-yl)imidazo[1,5-a]pyridine)₂(NMe₂)₂; In toluene; at 120 ℃; for 24h; Inert atmosphere; Sealed tube;

With lithium aluminium tetrahydride; In toluene; at 0 - 60 ℃; for 12h; Overall yield = 72 %; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c4ra14692a