5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

Base Information

Chemical Name:5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide
CAS No.:787629-28-1
Molecular Formula:C₄₈H₇₀N₆O₉
Molecular Weight:875.119
Hs Code.:

Synonyms:5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

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Chemical Property of 5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

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Technology Process of 5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

There total 5 articles about 5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 255062-86-3
2-octyloxybenzoic acid hydrazide

: 787629-28-1
5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / DCC / CH₂Cl₂ / 3 h / 20 °C

2: 94 percent / hydrazine hydrate / methanol / 2 h / 40 °C

3: 83 percent / EDCI / CH₂Cl₂ / 3 h / 20 °C

4: 70 percent / hydrazine hydrate / methanol; tetrahydrofuran / 4 h / 40 °C

With hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja047436p

Reference yield:

: 255062-85-2
2-octyloxybenzoic acid methyl ester

: 787629-28-1
5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / hydrazine hydrate / methanol / 5 h / 40 °C

2: 88 percent / DCC / CH₂Cl₂ / 3 h / 20 °C

3: 94 percent / hydrazine hydrate / methanol / 2 h / 40 °C

4: 83 percent / EDCI / CH₂Cl₂ / 3 h / 20 °C

5: 70 percent / hydrazine hydrate / methanol; tetrahydrofuran / 4 h / 40 °C

With hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja047436p

Reference yield:

: 267897-57-4
dimethyl 4,6-bis(octyloxy)-1,3-benzenedicarboxylate

: 787629-28-1
5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / KOH / dimethylsulfoxide / 2 h / 130 °C

2: 83 percent / EDCI / CH₂Cl₂ / 3 h / 20 °C

3: 70 percent / hydrazine hydrate / methanol; tetrahydrofuran / 4 h / 40 °C

With potassium hydroxide; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja047436p