C₅₈H₉₄O₁₇Si₃

Base Information

Chemical Name:C₅₈H₉₄O₁₇Si₃
CAS No.:131681-83-9
Molecular Formula:C₅₈H₉₄O₁₇Si₃
Molecular Weight:1147.63
Hs Code.:

C<sub>58</sub>H<sub>94</sub>O<sub>17</sub>Si<sub>3</sub>

Synonyms:C₅₈H₉₄O₁₇Si₃

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Chemical Property of C₅₈H₉₄O₁₇Si₃

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Technology Process of C₅₈H₉₄O₁₇Si₃

There total 27 articles about C₅₈H₉₄O₁₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 106711-69-7,106759-94-8,134357-84-9
C₄₉H₈₈O₁₆Si₃

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 131681-83-9
C₅₈H₉₄O₁₇Si₃

Guidance literature:: With pyridine; 4-pyrrolidin-1-ylpyridine; triethylamine; for 20h; Ambient temperature;

Reference yield:

: 18439-45-7,70632-45-0,87938-30-5,18439-44-6
3-O-Benzyl-6-desoxy-1,2-O-isopropyliden-α-D-gluco-hexofuranose

: 131681-83-9
C₅₈H₉₄O₁₇Si₃

Guidance literature:: Multi-step reaction with 15 steps

1: 94 percent / 2 N H₂SO₄ / tetrahydrofuran / 48 h / 60 °C

2: 65 percent / camphorsulfonic acid (CSA) / tetrahydrofuran / 1.) rt, 20 h, 2.) 60 deg C, 6 h

3: 99 percent / DMAP, pyridine / CH₂Cl₂ / 0.33 h

4: camphorsulfonic acid (CSA) / benzene / 27 h / Heating

5: 75 percent / Hg(CN)2, 4A molecular sieves / benzene / 1 h / Ambient temperature

6: 73 percent / 10percent Pd/C / methanol / 4 h / Heating

7: K₂CO₃ / methanol; tetrahydrofuran / 23 h / Ambient temperature

8: DMAP, Et₃N / dimethylformamide / 12 h / Ambient temperature

9: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C, 2.) from -78 deg C to rt

10: 88 percent / H₂ / 10percent Pd/C / ethyl acetate / Ambient temperature

11: 96 percent / 4-pyrrolidinopyridine, Et₃N / 4.5 h / Ambient temperature

12: 100 percent / Et₃N / methanol / 23 h / Ambient temperature

13: Ph₃P (TPP), diisopropyl azodicarboxylate (DIAD) / tetrahydrofuran / 27 h / Ambient temperature

14: 83 percent / NaBH₄ / methanol; tetrahydrofuran / 0.08 h / -20 °C

15: 91 percent / 4-pyrrolidinopyridine, pyridine, Et₃N / 20 h / Ambient temperature

With pyridine; dmap; sodium tetrahydroborate; di-isopropyl azodicarboxylate; 4 A molecular sieve; sulfuric acid; camphor-10-sulfonic acid; hydrogen; mercury(II) cyanide; potassium carbonate; 4-pyrrolidin-1-ylpyridine; ozone; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;

Reference yield:

: 106711-50-6,134311-77-6
3-O-Benzyl-6-deoxy-D-glucose

: 131681-83-9
C₅₈H₉₄O₁₇Si₃

Guidance literature:: Multi-step reaction with 14 steps

1: 65 percent / camphorsulfonic acid (CSA) / tetrahydrofuran / 1.) rt, 20 h, 2.) 60 deg C, 6 h

2: 99 percent / DMAP, pyridine / CH₂Cl₂ / 0.33 h

3: camphorsulfonic acid (CSA) / benzene / 27 h / Heating

4: 75 percent / Hg(CN)2, 4A molecular sieves / benzene / 1 h / Ambient temperature

5: 73 percent / 10percent Pd/C / methanol / 4 h / Heating

6: K₂CO₃ / methanol; tetrahydrofuran / 23 h / Ambient temperature

7: DMAP, Et₃N / dimethylformamide / 12 h / Ambient temperature

8: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C, 2.) from -78 deg C to rt

9: 88 percent / H₂ / 10percent Pd/C / ethyl acetate / Ambient temperature

10: 96 percent / 4-pyrrolidinopyridine, Et₃N / 4.5 h / Ambient temperature

11: 100 percent / Et₃N / methanol / 23 h / Ambient temperature

12: Ph₃P (TPP), diisopropyl azodicarboxylate (DIAD) / tetrahydrofuran / 27 h / Ambient temperature

13: 83 percent / NaBH₄ / methanol; tetrahydrofuran / 0.08 h / -20 °C

14: 91 percent / 4-pyrrolidinopyridine, pyridine, Et₃N / 20 h / Ambient temperature

With pyridine; dmap; sodium tetrahydroborate; di-isopropyl azodicarboxylate; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; mercury(II) cyanide; potassium carbonate; 4-pyrrolidin-1-ylpyridine; ozone; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;