D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate

Base Information

Chemical Name:D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate
CAS No.:1443793-24-5
Molecular Formula:C₂HF₃O₂*C₃₂H₄₃N₅O₁₁S
Molecular Weight:819.81
Hs Code.:

Synonyms:D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate

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Chemical Property of D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate

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Technology Process of D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate

There total 14 articles about D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: C₄₀H₅₅N₅O₁₃S

: 1443793-24-5
D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate

Guidance literature:: With water; trifluoroacetic acid; In acetonitrile; at 20 ℃; for 0.25h;
DOI:10.1021/jo4007893

Reference yield:

: 69489-40-3
D-2-[p-(benzyloxy)phenyl]glycine

: 1443793-24-5
D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / water; tetrahydrofuran / 12 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.02 h / 0 °C

2.2: 3 h / 0 - 20 °C

3.1: pyridine / 12 h / 20 °C

4.1: 10 wt% Pd(OH)2 on carbon; hydrogen / tetrahydrofuran / 12 h / 2585.81 Torr

5.1: potassium carbonate; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0 - 20 °C

6.1: trifluoroacetic acid; water / acetonitrile / 0.25 h / 20 °C

With pyridine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; 10 wt% Pd(OH)2 on carbon; water; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo4007893

Reference yield:

: 1443793-01-8
N-tert-butyloxycarbonyl-L-serine-D-[p-(benzyloxy)phenyl]glycine benzyl ester

: 1443793-24-5
D-(p-hydroxyphenyl)glycine-L-acetylserine-L-(p-hydroxyphenyl)glycylpantetheine trifluoroacetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.02 h / 0 °C

2.2: 3 h / 0 - 20 °C

3.1: pyridine / 12 h / 20 °C

4.1: 10 wt% Pd(OH)2 on carbon; hydrogen / tetrahydrofuran / 12 h / 2585.81 Torr

5.1: potassium carbonate; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0 - 20 °C

6.1: trifluoroacetic acid; water / acetonitrile / 0.25 h / 20 °C

With pyridine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; 10 wt% Pd(OH)2 on carbon; water; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo4007893