4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene

Base Information

Chemical Name:4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene
CAS No.:1204222-73-0
Molecular Formula:C₁₆H₁₄BrCl
Molecular Weight:324.62
Hs Code.:

Synonyms:4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene

Chemical Property:

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Technology Process of 4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene

There total 8 articles about 4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1204222-71-8
4-bromo-1-chloro-2-(4-(cyclopropyl-1-d)benzyl)benzene

: 1204222-73-0
4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene

Guidance literature:: With tetrabutylammonium bisulfate; water-d2; sodium hydride; In hexane; mineral oil; at 0 - 25 ℃;

Reference yield:

: 23088-37-1
2,2-d₂-phenethyl bromide

: 1204222-73-0
4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-benzyl-N,N,N-triethylammonium chloride; potassium hydroxide / dichloromethane / 19 h / Reflux

1.2: 5 h

1.3: 12 h / Reflux

2.1: aluminum (III) chloride / dichloromethane / 0 - 25 °C

3.1: trifluorormethanesulfonic acid; trifluoroacetic acid / 5 h / 25 °C

4.1: ammonium chloride; zinc / methanol / 8 h / Reflux

5.1: tetrabutylammonium bisulfate; water-d2; sodium hydride / hexane; mineral oil / 0 - 25 °C

With aluminum (III) chloride; trifluorormethanesulfonic acid; tetrabutylammonium bisulfate; N-benzyl-N,N,N-triethylammonium chloride; water-d2; sodium hydride; ammonium chloride; trifluoroacetic acid; potassium hydroxide; zinc; In methanol; hexane; dichloromethane; mineral oil;

Reference yield:

: 1204222-65-0
(2,2-dibromocyclopropyl-1-d)benzene

: 1204222-73-0
4-bromo-1-chloro-2-((4-(cyclopropyl-1-d)phenyl)methyl-d2)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / dichloromethane / 0 - 25 °C

2: trifluorormethanesulfonic acid; trifluoroacetic acid / 5 h / 25 °C

3: ammonium chloride; zinc / methanol / 8 h / Reflux

4: tetrabutylammonium bisulfate; water-d2; sodium hydride / hexane; mineral oil / 0 - 25 °C

With aluminum (III) chloride; trifluorormethanesulfonic acid; tetrabutylammonium bisulfate; water-d2; sodium hydride; ammonium chloride; trifluoroacetic acid; zinc; In methanol; hexane; dichloromethane; mineral oil;