2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide

Base Information

• Chemical Name: 2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide
• CAS No.: 1265576-48-4
• Molecular Formula: C₁₆H₁₇N₇OS₂
• Molecular Weight: 387.489

Synonyms:2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide

Chemical Property of 2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide

There total 2 articles about 2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.5%

2-(5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidin-2-ylthio)acetohydrazide (351176-83-5) + phenyl isothiocyanate (103-72-0) → 2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide (1265576-48-4)

Guidance literature:

In ethanol; for 8h; Reflux;

Reference yield:

2-ethoxyacetylthio-5,7-dimethyl-1,2,4-triazolo[1,5-a]pyrimidine (351176-82-4) → 2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide (1265576-48-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / water

2: ethanol / 8 h / Reflux

With hydrazine hydrate; In ethanol; water;

Reference yield: 97.3%

2-(2-(5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)acetyl)-N-phenylhydrazinecarbothioamide (1265576-48-4) → 5-((5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidin-2-ylthio)methyl)-4-phenyl-4H-1, 2,4-triazole-3-thiol (936099-29-5)

Guidance literature:

With sodium carbonate; In water; for 4h; Reflux;

upstream raw materials:

2-ethoxyacetylthio-5,7-dimethyl-1,2,4-triazolo[1,5-a]pyrimidine

2-(5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidin-2-ylthio)acetohydrazide

phenyl isothiocyanate

Downstream raw materials:

2-[(5-(2-bromobenzylthio)-4-phenyl-4H-1,2,4-triazol-3-yl)methylthio]-5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidine

2-[(5-(3-bromobenzylthio)-4-phenyl-4H-1,2,4-triazol-3-yl)methylthio]-5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidine

2-[(5-(4-bromobenzylthio)-4-phenyl-4H-1,2,4-triazol-3-yl)methylthio]-5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidine

2-[(5-(2-fluorobenzylthio)-4-phenyl-4H-1,2,4-triazol-3-yl)methylthio]-5,7-dimethyl-[1,2,4]triazolo[1,5-α]pyrimidine

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