benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate

Base Information

Chemical Name:benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate
CAS No.:1207461-43-5
Molecular Formula:C₂₂H₃₅NO₃Si
Molecular Weight:389.61
Hs Code.:

Synonyms:benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate

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Technology Process of benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate

There total 1 articles about benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1207461-44-6
benzyl (R)-allyl[7-(tert-butyldimethylsilyloxy)-1-hepten-4-yl]carbamate

: 1207461-43-5
benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol902920u

Reference yield: 83.0%

: 1207461-43-5
benzyl (R)-6-[3-(tert-butyldimethylsilyloxy)propyl]-5,6-dihydro-1(2H)-pyridinecarboxylate

: 1207461-47-9
benzyl (1S,4R,6R)-4-[3-(tert-butyldimethylsilyloxy)propyl]-7-oxa-3-azabicyclo[4.1.0]heptane-3-carboxylate

Guidance literature:: With Oxone; 1,1,1-trifluoro-2-propanone; disodium ethylenediaminetetraacetic acid; sodium hydrogencarbonate; In water; acetonitrile; at 0 - 20 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol902920u