α-Butoxycyclohexanon

Base Information

Chemical Name:α-Butoxycyclohexanon
CAS No.:33371-99-2
Molecular Formula:C₁₀H₁₈O₂
Molecular Weight:170.252
Hs Code.:

Synonyms:α-Butoxycyclohexanon

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-Butoxycyclohexanon

Chemical Property:

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Technology Process of α-Butoxycyclohexanon

There total 1 articles about α-Butoxycyclohexanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33371-99-2
α-Butoxycyclohexanon

Guidance literature:: Alkohol I, n-Butanol;

Reference yield: 34.4%

: 33371-99-2
α-Butoxycyclohexanon

: 76899-07-5,78963-47-0,78963-48-1,78963-60-7,80951-41-3,81275-02-7,85647-75-2,85954-95-6,92217-74-8,104527-11-9,76855-69-1
(3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one

: 950187-51-6
3-(S)-[1-(R)-(tert-butyldimethylsilyloxy)-ethyl]-4-(R)-((1S,3R)-3-butoxy-2-oxo-cyclohexyl)-azetidin-2-one

: 950187-52-7
3-(S)-[1-(R)-(tert-butyldimethylsilyloxy)-ethyl]-4-(R)-((1R,3S)-3-butoxy-2-oxo-cyclohexyl)-azetidin-2-one

Guidance literature:: α-Butoxycyclohexanon; With tin(IV) chloride; In dichloromethane; at -20 ℃; for 0.25h;

(3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one; In dichloromethane; at 0 ℃; for 1h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 1h; Further stages.;
DOI:10.1021/jm0703237

Reference yield:

: 33371-99-2
α-Butoxycyclohexanon

: 950187-53-8
3-(S)-[1-(R)-(tert-butyldimethylsilyloxy)-ethyl]-4-(R)-((1S)-3-(R)-butoxy-2-oxo-cyclohexyl)-allyloxalyl-azetidin-2-on

Guidance literature:: Multi-step reaction with 2 steps

1.1: SnCl₄ / CH₂Cl₂ / 0.25 h / -20 °C

1.2: CH₂Cl₂ / 1 h / 0 °C

1.3: 34.4 percent / ethyl diisopropylamine / CH₂Cl₂ / 1 h / 0 °C

2.1: 79.7 percent / Et₃N / tetrahydrofuran / 2.5 h / -5 - 20 °C

With tin(IV) chloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0703237