13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane)

Base Information

Chemical Name:13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane)
CAS No.:1012326-22-5
Molecular Formula:C₂₄H₄₀I₂O₁₀
Molecular Weight:742.385
Hs Code.:

Synonyms:13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane)

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Technology Process of 13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane)

There total 1 articles about 13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 110429-45-3,92450-98-1
1-{2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy}-2-methoxy-ethane

: 361525-84-0
1,4-diiodo-2,3-dihydroxybenzene

: 1012326-22-5
13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane)

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetonitrile; for 18h; Heating;
DOI:10.1021/jo702380b

Reference yield: 86.0%

: 1012326-22-5
13,13'-(3,6-diiodo-1,2-phenylene)bis(oxy)bis(2,5,8,11-tetraoxatridecane)

: 4-ethynylpyridine hydrochloride

: 1012326-28-1
4,4'-(2,3-bis(2,5,8,11-tetraoxatridecan-13-yloxy)-1,4-phenylene)bis(ethyne-2,1-diyl)dipyridine

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 36h;
DOI:10.1021/jo702380b