C₁₄H₂₁IO

Base Information

Chemical Name:C₁₄H₂₁IO
CAS No.:1620643-52-8
Molecular Formula:C₁₄H₂₁IO
Molecular Weight:332.225
Hs Code.:

Synonyms:C₁₄H₂₁IO

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Chemical Property of C₁₄H₂₁IO

Chemical Property:

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Technology Process of C₁₄H₂₁IO

There total 1 articles about C₁₄H₂₁IO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 169105-68-4
(2S,4S)-5-benzyloxy-2,4-dimethyl-pentan-1-ol

: 1620643-52-8
C₁₄H₂₁IO

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In diethyl ether; acetonitrile; at 0 - 20 ℃; for 13h; Inert atmosphere;
DOI:10.1002/anie.201400305

Reference yield:

: 1620643-52-8
C₁₄H₂₁IO

: C₄₄H₈₀O₆Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: dimethyl sulfoxide / 39 h / 20 °C / Inert atmosphere

2.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 2 h / 20 °C / Inert atmosphere

3.1: triphenylphosphine; 1H-imidazole; iodine / diethyl ether; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 °C / Inert atmosphere

5.1: propionic acid; pyrrolidine / water; isopropyl alcohol / 18 h / 55 °C / Inert atmosphere

6.1: cerium(III) chloride heptahydrate / ethanol / 0.5 h / 0 °C / Inert atmosphere

6.2: 2 h / 0 °C / Inert atmosphere

7.1: 1H-imidazole / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

8.1: tert.-butyl lithium / diethyl ether; pentane / 0.08 h / -78 °C / Inert atmosphere

8.2: 4 h / 20 °C / Inert atmosphere

9.1: Schwartz's reagent / benzene / 24 h / 20 °C / Inert atmosphere

9.2: 1 h

9.3: 20 h / 20 °C / Darkness

With pyrrolidine; 1H-imidazole; Schwartz's reagent; chloro-trimethyl-silane; cerium(III) chloride heptahydrate; iodine; tert.-butyl lithium; diisobutylaluminium hydride; propionic acid; triphenylphosphine; sodium iodide; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; acetonitrile; pentane; benzene; 9.3: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201400305

Reference yield:

: 1620643-52-8
C₁₄H₂₁IO

: C₄₆H₈₄O₇Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: dimethyl sulfoxide / 39 h / 20 °C / Inert atmosphere

2.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 2 h / 20 °C / Inert atmosphere

3.1: triphenylphosphine; 1H-imidazole; iodine / diethyl ether; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 °C / Inert atmosphere

5.1: propionic acid; pyrrolidine / water; isopropyl alcohol / 18 h / 55 °C / Inert atmosphere

6.1: cerium(III) chloride heptahydrate / ethanol / 0.5 h / 0 °C / Inert atmosphere

6.2: 2 h / 0 °C / Inert atmosphere

7.1: 1H-imidazole / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

8.1: tert.-butyl lithium / diethyl ether; pentane / 0.08 h / -78 °C / Inert atmosphere

8.2: 4 h / 20 °C / Inert atmosphere

9.1: Schwartz's reagent / benzene / 24 h / 20 °C / Inert atmosphere

9.2: 1 h

9.3: 20 h / 20 °C / Darkness

10.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

10.2: 1 h / 20 °C / Inert atmosphere

With pyrrolidine; 1H-imidazole; Schwartz's reagent; chloro-trimethyl-silane; cerium(III) chloride heptahydrate; iodine; tert.-butyl lithium; sodium hydride; diisobutylaluminium hydride; propionic acid; triphenylphosphine; sodium iodide; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; acetonitrile; mineral oil; pentane; benzene; 9.3: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201400305