2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin

Base Information

• Chemical Name: 2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin
• CAS No.: 76734-99-1
• Molecular Formula: C₂₀H₂₂N₂O₆
• Molecular Weight: 386.404
• Mol file: 76734-99-1.mol

Synonyms:2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin

Chemical Property of 2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin

There total 1 articles about 2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-acetyldopamine (2494-12-4) → 2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin (76734-99-1)

Guidance literature:

With Locusta migratoria; oxygen; edetate disodium; Ambient temperature; 0.2M Na-acetate buffer, pH 5.5, overnight incubation;

DOI:10.1016/0040-4020(80)80172-4

Reference yield:

2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin (76734-99-1) → dopamine (51-61-6) + arterenone (499-61-6) + 2-hydroxy-3′,4′-dihydroxyacetophenone (29477-54-1)

Guidance literature:

With hydrogenchloride; at 110 ℃; for 3h;

DOI:10.1016/0040-4020(80)80172-4

Reference yield:

2-(3',4'-dihydroxyphenyl)-3-acetylamino-6-(N-acetyl-2''-aminoethyl)-2,3-dihydro-1,4-benzodioxin (76734-99-1) → dopamine (51-61-6) + 2-hydroxy-3′,4′-dihydroxyacetophenone (29477-54-1)

Guidance literature:

With hydrogenchloride; for 3h; Heating;

DOI:10.1016/0040-4020(80)80172-4

upstream raw materials:

N-acetyldopamine

Downstream raw materials:

dopamine

arterenone

2-hydroxy-3′,4′-dihydroxyacetophenone

N-acetyldopamine