2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid

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Chemical Name:2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid
CAS No.:1393097-70-5
Molecular Formula:C₁₆H₈ClF₈N₅O₂
Molecular Weight:489.712
Hs Code.:

Synonyms:2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid

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Chemical Property of 2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid

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Technology Process of 2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid

There total 8 articles about 2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104315-28-8
5-fluoro-1-methyl-3-(1,1,2,2,2-pentafluoroethyl)-4-(trifluoromethyl)pyrazole

: 1393097-70-5
2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / dimethyl sulfoxide / 20 °C

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

3: water; lithium hydroxide / tetrahydrofuran / 5 h / 60 °C

With sodium azide; water; lithium hydroxide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; dimethyl sulfoxide; tert-butyl alcohol;

Reference yield:

: 1382041-61-3
5-azido-1-methyl-3-(1,1,2,2,2-pentafluoroethyl)-4-(trifluoromethyl)pyrazole

: 1393097-70-5
2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

2: water; lithium hydroxide / tetrahydrofuran / 5 h / 60 °C

With water; lithium hydroxide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; tert-butyl alcohol;

Reference yield:

: 1584-03-8
perfluoro-2-methylpent-2-ene

: 1393097-70-5
2-chloro-5-[1-(2-methyL-5-(pentafluoroethyl)-4-(trifluoromethyl)-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane; water / 0 - 20 °C

2: sodium azide / dimethyl sulfoxide / 20 °C

3: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

4: water; lithium hydroxide / tetrahydrofuran / 5 h / 60 °C

With sodium azide; copper(ll) sulfate pentahydrate; water; sodium L-ascorbate; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;