Technology Process of C9H7IOTe
There total 5 articles about C9H7IOTe which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
acetone;
at 50 ℃;
for 0.25h;
DOI:10.1021/ja00342a040
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) sodium borohydride / 1.) THF, ethanol, 2.) room temperature, 0.5 h
2: 82 percent / aq. potassium hydroxide / ethanol / 1 h / 50 °C
3: oxalyl chloride
4: 82 percent / aluminum chloride / CH2Cl2 / -78 deg C -> room temperature
5: 75 percent / sodium iodide / acetone / 0.25 h / 50 °C
With
potassium hydroxide; sodium tetrahydroborate; aluminium trichloride; oxalyl dichloride; sodium iodide;
In
ethanol; dichloromethane; acetone;
DOI:10.1021/ja00342a040
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 82 percent / aq. potassium hydroxide / ethanol / 1 h / 50 °C
2: oxalyl chloride
3: 82 percent / aluminum chloride / CH2Cl2 / -78 deg C -> room temperature
4: 75 percent / sodium iodide / acetone / 0.25 h / 50 °C
With
potassium hydroxide; aluminium trichloride; oxalyl dichloride; sodium iodide;
In
ethanol; dichloromethane; acetone;
DOI:10.1021/ja00342a040