Technology Process of C23H37NO3Si
There total 1 articles about C23H37NO3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
diethyl ether; Petroleum ether;
at -30 ℃;
for 24h;
DOI:10.1002/ejoc.200601011
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 78 percent / hydrogen / Pd/C / ethanol / 12 h / 20 °C / atmospheric pressure
2.1: 86 percent / iPr2NEt / CH2Cl2 / 15 h / 20 °C
3.1: 95 percent / CF3COOH / methanol; H2O / 15 h / 20 °C
4.1: NaIO4 / methanol / 3 h / 20 °C
4.2: Jones' reagent / acetone / 4 h / 0 °C
With
sodium periodate; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; ethanol; dichloromethane; water;
DOI:10.1002/ejoc.200601011
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / hydrogen / Pd/C / ethanol / 12 h / 20 °C / atmospheric pressure
2: 86 percent / iPr2NEt / CH2Cl2 / 15 h / 20 °C
With
hydrogen; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
ethanol; dichloromethane;
DOI:10.1002/ejoc.200601011