Technology Process of [((2,2'-bipyridine)(acetylacetonato)Ru(II))2(μ-2,5-dihydroxy-1,4-benzoquinone(2-))]
There total 1 articles about [((2,2'-bipyridine)(acetylacetonato)Ru(II))2(μ-2,5-dihydroxy-1,4-benzoquinone(2-))] which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
ethylene glycol;
byproducts: KBr; a mixt. of a ligand (0.25 mmol) and Ru-contg. compd. (0.5 mmol) in ethylene glycol was heated in a water bath for 1 h; cooling; sepn. of the complex; it was centrifuged and dried in vac.; it was dissolved in CH2Cl2 to remove KBr; CH2Cl2 evapg. at room temp.; the complex was washed with ethanol and dried in vac.; elem. anal.;