[7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime

Base Information

Chemical Name:[7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime
CAS No.:949530-35-2
Molecular Formula:C₁₉H₂₅NO₃
Molecular Weight:315.412
Hs Code.:

Synonyms:[7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime

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Chemical Property of [7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime

Chemical Property:

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Technology Process of [7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime

There total 7 articles about [7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949530-33-0
[7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde

: 949530-35-2
[7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime

Guidance literature:: With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; water; for 18h; Heating;
DOI:10.1021/ol071049d

Reference yield:

: 7-(4-methoxyphenyl)spiro[4.5]decan-6-ol

: 949530-35-2
[7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: 61 percent / PDC / benzene / Heating

2.1: 89 percent / potassium tert-butoxide / toluene / 24 h / Heating

3.1: O₃ / CH₂Cl₂ / 1 h / -78 °C

3.2: 80 percent / dimethyl sulfide / CH₂Cl₂ / 20 °C

4.1: NH₂OH*HCl; NaOH / ethanol; H₂O / 18 h / Heating

With sodium hydroxide; dipyridinium dichromate; hydroxylamine hydrochloride; potassium tert-butylate; ozone; In ethanol; dichloromethane; water; toluene; benzene;
DOI:10.1021/ol071049d

Reference yield:

: N-[(6E)-spiro[4.5]dec-6-ylidene]benzenesulfonhydrazide

: 949530-35-2
[7-(4-methoxyphenyl)-6-oxo-spiro[4.5]dec-7-yl]acetaldehyde oxime

Guidance literature:: Multi-step reaction with 7 steps

1.1: 81 percent / sodium methoxide / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating

2.1: 97 percent / mCPBA; NaHCO₃ / diethyl ether / 0.17 h

3.1: CuCN / diethyl ether / 0.17 h / -78 °C

3.2: 49 percent / BF₃*Et₂O / diethyl ether / 20 °C

4.1: 61 percent / PDC / benzene / Heating

5.1: 89 percent / potassium tert-butoxide / toluene / 24 h / Heating

6.1: O₃ / CH₂Cl₂ / 1 h / -78 °C

6.2: 80 percent / dimethyl sulfide / CH₂Cl₂ / 20 °C

7.1: NH₂OH*HCl; NaOH / ethanol; H₂O / 18 h / Heating

With sodium hydroxide; dipyridinium dichromate; hydroxylamine hydrochloride; potassium tert-butylate; sodium methylate; sodium hydrogencarbonate; ozone; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; ethanol; dichloromethane; diethylene glycol dimethyl ether; water; toluene; benzene;
DOI:10.1021/ol071049d