phenylthalium(III) di(trifluoroacetate)

Base Information Edit

Chemical Name:phenylthalium(III) di(trifluoroacetate)
CAS No.:23586-54-1
Molecular Formula:C₁₀H₅F₆O₄Tl
Molecular Weight:507.521
Hs Code.:
Mol file:23586-54-1.mol

Synonyms:phenylthalium(III) di(trifluoroacetate)

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Chemical Property of phenylthalium(III) di(trifluoroacetate) Edit

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Technology Process of phenylthalium(III) di(trifluoroacetate)

There total 2 articles about phenylthalium(III) di(trifluoroacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.5%

: thallium(III) trifluoroacetate

: 23586-54-1
phenylthalium(III) di(trifluoroacetate)

Guidance literature:: With benzene; In trifluoroacetic acid; according to McKillop, A., et al., Tetrahedron Lett., 1969, 2423;

Reference yield:

: thallium (III) oxide

: 76-05-1
trifluoroacetic acid

: 23586-54-1
phenylthalium(III) di(trifluoroacetate)

Guidance literature:: With benzene; In further solvent(s); Tl2O3 and CF3COOH refluxed with stirring in the dark for 75 h, cooled to room temp., filtered, benzene added, soln. stirred for 15 h at room temp., cooled to 0°C; precipitate filtered, washed with cold benzene, dried in vacuo over NaOH, elem. anal., IR, PMR;