3,3-⁽²⁾H₂-allyl toluene-4-sulfonate

Base Information

• Chemical Name: 3,3-⁽²⁾H₂-allyl toluene-4-sulfonate
• CAS No.: 108957-10-4
• Molecular Formula: C₁₀H₁₂O₃S
• Molecular Weight: 214.254
• Mol file: 108957-10-4.mol

Synonyms:3,3-⁽²⁾H₂-allyl toluene-4-sulfonate

Chemical Property of 3,3-⁽²⁾H₂-allyl toluene-4-sulfonate

Chemical Property:

Purity/Quality:

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Technology Process of 3,3-⁽²⁾H₂-allyl toluene-4-sulfonate

There total 1 articles about 3,3-⁽²⁾H₂-allyl toluene-4-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyl-3,3-d2 alcohol (1204699-10-4) + p-toluenesulfonyl chloride (98-59-9) → 3,3-(2)H2-allyl toluene-4-sulfonate (108957-10-4)

Guidance literature:

With dmap; triethylamine; In diethyl ether; at 20 ℃; for 14h; Inert atmosphere;

DOI:10.1021/jacs.1c12490

Reference yield:

3,3-(2)H2-allyl toluene-4-sulfonate (108957-10-4) + lithium triphenylstannide (4167-90-2) → 3,3-dideuterioallyl(triphenyl)stannane (37499-52-8,37590-87-7)

Guidance literature:

In tetrahydrofuran; -20°C;

DOI:10.1039/c39860001339

upstream raw materials:

allyl-3,3-d₂ alcohol

p-toluenesulfonyl chloride

Downstream raw materials:

3,3-dideuterioallyl(triphenyl)stannane