2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril

Base Information

• Chemical Name: 2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril
• CAS No.: 97847-93-3
• Molecular Formula: C₁₉H₂₀F₃NOSi
• Molecular Weight: 363.455

Synonyms:2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril

Chemical Property of 2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril

Chemical Property:

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Technology Process of 2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril

There total 1 articles about 2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

tropylium tetrafluoroborate (27081-10-3) + 2-(4-(trifluoromethyl)phenyl)-2-((trimethylsilyl)oxy)acetonitrile (73183-23-0) → 2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril (97847-93-3)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; - 78 deg C to r.t.;

Reference yield: 65.0%

2,4,6-Cycloheptatrien-1-yl<4-(trifluormethyl)phenyl>(trimethylsiloxy)acetonitril (97847-93-3) → 2,4,6-Cycloheptatrien-1-yl-<4-(trifluormethyl)phenyl>keton (97847-95-5)

Guidance literature:

With triethylamine hydrofluoride;

DOI:10.1016/S0040-4039(00)94871-8

upstream raw materials:

tropylium tetrafluoroborate

2-(4-(trifluoromethyl)phenyl)-2-((trimethylsilyl)oxy)acetonitrile

Downstream raw materials:

2,4,6-Cycloheptatrien-1-yl-<4-(trifluormethyl)phenyl>keton

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