2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol

Base Information

Chemical Name:2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol
CAS No.:160083-34-1
Molecular Formula:C₃₂H₄₀O₁₉S
Molecular Weight:760.724
Hs Code.:

Synonyms:2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol

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Chemical Property of 2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol

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Technology Process of 2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol

There total 1 articles about 2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68636-40-8
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranose

: 106-51-4
p-benzoquinone

: 160083-34-1
2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol

Guidance literature:: With sodium dithionite; Yield given. Multistep reaction; 1.) MeOH, THF, 1 h, r.t., 2.) CH₃Cl, H₂O, 5 min, r.t.;
DOI:10.1002/hlca.19940770319

Reference yield: 70.0%

: 160083-34-1
2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol

: 160083-35-2
2-(β-D-cellobiosylthio)benzene-1,4-diol

Guidance literature:: With sodium methylate; In methanol; for 3h; Ambient temperature;
DOI:10.1002/hlca.19940770319

Reference yield:

: 160083-34-1
2-(2',2'',3',3'',4'',6',6''-hepta-O-acetyl-β-D-cellobiosylthio)benzene-1,4-diol

: 2-(β-D-cellobiosylthio)benzo-1,4-quinone

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaOMe / methanol / 3 h / Ambient temperature

2: 75 percent / PhI(OAc)2 / methanol / 0.33 h / Ambient temperature

With [bis(acetoxy)iodo]benzene; sodium methylate; In methanol;
DOI:10.1002/hlca.19940770319