2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde

Base Information

Chemical Name:2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde
CAS No.:88180-33-0
Molecular Formula:C₁₅H₁₆O₄
Molecular Weight:260.29
Hs Code.:

Synonyms:2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde

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Chemical Property of 2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde

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Technology Process of 2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde

There total 3 articles about 2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 72233-96-6
N,N-Dimethyl(4',6'-O-benzylidene-2',3'-dideoxy-α-D-erythro-hex-2'-enopyranosyl)acetamide

: 88200-24-2
2-(4',6'-O-Benzylidene-2',3'-dideoxy-α-D-erythro-hex-2'-enopyranosyl)acetaldehyde

: 88180-33-0
2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde

Guidance literature:: With lithium triethoxyaluminum hydride; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1021/jo00177a026

Reference yield:

: 63598-38-9,167074-37-5
1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-ribo-hex-1-enopyranose

: 88180-33-0
2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / xylene / 2 h / Heating

2: 90 percent / Li(OC₂H₅)3AlH / diethyl ether / 1 h / 0 °C

With lithium triethoxyaluminum hydride; In diethyl ether; xylene;
DOI:10.1021/jo00177a026

Reference yield:

: 88180-35-2
C₁₉H₂₆NO₄⁽¹⁺⁾*BF₄^(1-)

: 88180-33-0
2-(4',6'-O-Benzylidene-2',3'-dideoxy-β-D-erythro-hex-2'-enopyranosyl)acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1N NaOH / benzonitrile; H₂O / 0.5 h

2: 90 percent / Li(OC₂H₅)3AlH / diethyl ether / 1 h / 0 °C

With sodium hydroxide; lithium triethoxyaluminum hydride; In diethyl ether; water; benzonitrile;
DOI:10.1021/jo00177a026