phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:869005-02-7
Molecular Formula:C₇₆H₇₃NO₁₇S
Molecular Weight:1304.48
Hs Code.:

phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Synonyms:phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 4 articles about phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 869004-99-9
phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 116514-50-2,128962-63-0,131545-02-3,136758-06-0,99409-34-4,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

: 869005-02-7
phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside; With 4 A molecular sieve; In toluene; at 20 ℃; for 0.5h;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In toluene; at -25 ℃;
DOI:10.1016/j.tetasy.2005.08.007

Reference yield:

: C₂₂H₂₂O₈

: 869005-02-7
phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 95 percent / DBU / CH₂Cl₂ / 1 h / 0 °C

2.1: molecular sieves 4 Angstroem / CH₂Cl₂ / 0.67 h / 20 °C

2.2: 75 percent / trimethylsilyl triflate / CH₂Cl₂ / 0 °C

3.1: molecular sieves 4 Angstroem / toluene / 0.5 h / 20 °C

3.2: 62 percent / N-iodosuccinimide; trifluoromethanesulfonic acid / toluene / -25 °C

With 4 A molecular sieve; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; toluene;
DOI:10.1016/j.tetasy.2005.08.007

Reference yield:

: 869004-95-5
4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylohexopyranosyl trichloroacetimidate

: 869005-02-7
phenyl(4-O-acetyl-2,6-di-O-benzoyl-3-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: molecular sieves 4 Angstroem / CH₂Cl₂ / 0.67 h / 20 °C

1.2: 75 percent / trimethylsilyl triflate / CH₂Cl₂ / 0 °C

2.1: molecular sieves 4 Angstroem / toluene / 0.5 h / 20 °C

2.2: 62 percent / N-iodosuccinimide; trifluoromethanesulfonic acid / toluene / -25 °C

With 4 A molecular sieve; In dichloromethane; toluene;
DOI:10.1016/j.tetasy.2005.08.007