benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

• Chemical Name: benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
• CAS No.: 1072107-86-8
• Molecular Formula: C₄₀H₄₅N₃O₁₀
• Molecular Weight: 727.811

Synonyms:benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Chemical Property of benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside → benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (1072107-86-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at -20 - 0 ℃; for 1.5h;

DOI:10.1021/ja805044x

Reference yield: 79.0%

benzyl 2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside (1072107-86-8) + 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl trichloroimidate (121238-27-5) → benzyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->4)]-{[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->6)]}-2-O-benzyl-β-D-mannopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja805044x

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