N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide

Base Information

Chemical Name:N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide
CAS No.:80535-07-5
Molecular Formula:C₁₆H₂₀F₃NO₂
Molecular Weight:315.336
Hs Code.:

Synonyms:N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide

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Chemical Property of N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide

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Technology Process of N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide

There total 8 articles about N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 62114-63-0
N-methyl metamethoxyphenyl-3 hexene-5 yl amine

: 407-25-0
trifluoroacetic anhydride

: 80535-07-5
N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide

Guidance literature:: With sodium carbonate;
DOI:10.1016/S0040-4020(01)92354-3

Reference yield:

: 6768-23-6
diethyl-2-(4-methoxybenzylidene)malonate

: 80535-07-5
N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Zn, dibromoethane / 1.) dibromoethane, THF, 55 deg C, 2 h; 2.) dibromoethane, THF, roomtemperature, 15 h

2: 85 percent / NaCl / dimethylsulfoxide; H₂O / 7 h / 200 °C

3: CH₃ONa / methanol / 96 h

4: 75 percent / LiAlH₄ / diethyl ether / 15 h / Heating

5: 96 percent / Na₂CO₃

With lithium aluminium tetrahydride; 1,1-Dibromoethane; sodium methylate; sodium carbonate; sodium chloride; zinc; In methanol; diethyl ether; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)92354-3

Reference yield:

: 80534-79-8
diethyl malonyl-1 metamethoxyphenyl-1 butene-3

: 80535-07-5
N-methyl metamethoxyphenyl-3 hexene-5 yl trifluoroacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / NaCl / dimethylsulfoxide; H₂O / 7 h / 200 °C

2: CH₃ONa / methanol / 96 h

3: 75 percent / LiAlH₄ / diethyl ether / 15 h / Heating

4: 96 percent / Na₂CO₃

With lithium aluminium tetrahydride; sodium methylate; sodium carbonate; sodium chloride; In methanol; diethyl ether; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)92354-3