benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester

Base Information

Chemical Name:benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester
CAS No.:512788-99-7
Molecular Formula:C₄₆H₅₀N₄O₁₁Si
Molecular Weight:863.009
Hs Code.:

benzoic acid 2,2-di-<i>tert</i>-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2<i>H</i>-pyrimidin-1-yl)-tetrahydro-furo[3,2-<i>d</i>][1,3,2]dioxasilin-7-yl ester

Synonyms:benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester

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Chemical Property of benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester

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Technology Process of benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester

There total 3 articles about benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 163889-34-7
N³-benzoyl-3',5'-O-(di-tert-butylsilanediyl)uridine

: 512788-95-3
C₂₂H₁₉IN₂O₄

: N³-benzoyl-3',5'-O-(di-tert-butylsilanediyl)-2'-O-benzoyluridine

: 512788-99-7
benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester

Guidance literature:: With benzyl dimethyl-perhydro-1,3,2-diazaphosphorine; tetra-(n-butyl)ammonium iodide; In acetonitrile; at 20 ℃; for 72h;
DOI:10.1081/NCN-120015728

Reference yield:

: 512789-04-7
C₂₂H₂₀N₂O₅

: 512788-99-7
benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / I₂; PPh₃; imidazole

2: 55 percent / benzyl dimethyl-perhydro-1,3,2-diazaphosphorine; mBu₄NI / acetonitrile / 72 h / 20 °C

With 1H-imidazole; benzyl dimethyl-perhydro-1,3,2-diazaphosphorine; iodine; tetra-(n-butyl)ammonium iodide; triphenylphosphine; In acetonitrile;
DOI:10.1081/NCN-120015728

Reference yield:

: 512789-03-6
C₂₂H₁₈N₂O₄

: 512788-99-7
benzoic acid 2,2-di-tert-butyl-6-(3-{4-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-butyl}-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furo[3,2-d][1,3,2]dioxasilin-7-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / BH₃; H₂O₂; alkali

2: 98 percent / I₂; PPh₃; imidazole

3: 55 percent / benzyl dimethyl-perhydro-1,3,2-diazaphosphorine; mBu₄NI / acetonitrile / 72 h / 20 °C

With 1H-imidazole; benzyl dimethyl-perhydro-1,3,2-diazaphosphorine; borane; dihydrogen peroxide; iodine; tetra-(n-butyl)ammonium iodide; triphenylphosphine; In acetonitrile;
DOI:10.1081/NCN-120015728