C₃₅H₅₀O₅Si

Base Information

Chemical Name:C₃₅H₅₀O₅Si
CAS No.:1591927-92-2
Molecular Formula:C₃₅H₅₀O₅Si
Molecular Weight:578.865
Hs Code.:

C<sub>35</sub>H<sub>50</sub>O<sub>5</sub>Si

Synonyms:C₃₅H₅₀O₅Si

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Chemical Property of C₃₅H₅₀O₅Si

Chemical Property:

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Technology Process of C₃₅H₅₀O₅Si

There total 7 articles about C₃₅H₅₀O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1591927-90-0
C₃₅H₄₈O₅Si

: 1591927-92-2
C₃₅H₅₀O₅Si

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -10 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol5008179

Reference yield:

: 1591927-86-4
C₃₂H₅₄O₄Si₂

: 1591927-92-2
C₃₅H₅₀O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: camphor-10-sulfonic acid / dichloromethane; methanol / 4 h / 0 - 20 °C / Inert atmosphere

2: camphor-10-sulfonic acid / dichloromethane; methanol / 2 h / 0 °C / Inert atmosphere

3: Proton-sponge / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

4: diisobutylaluminium hydride / dichloromethane; toluene / -10 °C / Inert atmosphere

With camphor-10-sulfonic acid; diisobutylaluminium hydride; In methanol; dichloromethane; toluene;
DOI:10.1021/ol5008179

Reference yield:

: 206255-62-1
4-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-butan-2-one

: 1591927-92-2
C₃₅H₅₀O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / diethyl ether / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / -95 - -78 °C / Inert atmosphere

3: tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 24 h / -40 - -30 °C / Inert atmosphere

4: camphor-10-sulfonic acid / dichloromethane; methanol / 4 h / 0 - 20 °C / Inert atmosphere

5: camphor-10-sulfonic acid / dichloromethane; methanol / 2 h / 0 °C / Inert atmosphere

6: Proton-sponge / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

7: diisobutylaluminium hydride / dichloromethane; toluene / -10 °C / Inert atmosphere

With camphor-10-sulfonic acid; boron trifluoride diethyl etherate; diisobutylaluminium hydride; triethylamine; tetramethylammonium triacetoxyborohydride; In methanol; diethyl ether; dichloromethane; acetic acid; toluene; acetonitrile; 2: |Mukaiyama Aldol Addition;
DOI:10.1021/ol5008179