Technology Process of C38H57F4N3O8SSi
There total 4 articles about C38H57F4N3O8SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen / palladium 10% on activated carbon / methanol / 760.05 Torr
2.1: caesium carbonate / dichloromethane / 16 h / 20 °C
3.1: water; lithium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C
3.2: 16 h / 20 °C
3.3: 2 h
4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 2 h
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: caesium carbonate / dichloromethane / 16 h / 20 °C
2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C
2.2: 16 h / 20 °C
2.3: 2 h
3.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 2 h
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; caesium carbonate; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
