C₃₈H₄₉IN₄O₇

Base Information

Chemical Name:C₃₈H₄₉IN₄O₇
CAS No.:950886-76-7
Molecular Formula:C₃₈H₄₉IN₄O₇
Molecular Weight:800.734
Hs Code.:

C<sub>38</sub>H<sub>49</sub>IN<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₈H₄₉IN₄O₇

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Chemical Property of C₃₈H₄₉IN₄O₇

Chemical Property:

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Technology Process of C₃₈H₄₉IN₄O₇

There total 12 articles about C₃₈H₄₉IN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: C₃₃H₄₇N₃O₈

: 615-43-0
2-iodophenylamine

: 950886-76-7
C₃₈H₄₉IN₄O₇

Guidance literature:: With trimethylaluminum; potassium carbonate; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2007.05.127

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 950886-76-7
C₃₈H₄₉IN₄O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: 33.4 g / Na₂CO₃ / dioxane; H₂O / 1.5 h / 20 °C

2.1: sodium borohydride; LiCl / tetrahydrofuran; ethanol / 5 h / 20 °C

3.1: 2.11 g / p-toluenesulfonic acid monohydrate / benzene / 3 h / 20 °C

4.1: s-BuLi; N,N,N',N'-tetramethylethylenediamine / diethyl ether; cyclohexane / 0.33 h / -78 °C

4.2: 73 percent / 1,2-diiodoethane / cyclohexane; diethyl ether / 0 - 20 °C

5.1: 47 percent / K₂CO₃; DDQ / benzene / 12 h / 70 °C

6.1: Bu₃SnH / Pd(PPh₃)4 / CH₂Cl₂ / -10 °C

6.2: copper(I) iodide; tri(2-furyl)phosphine / Pd₂(dba)3*CHCl₃ / 1-methyl-pyrrolidin-2-one

7.1: 82 percent / DMSO / 130 °C

8.1: 93 percent / Me₃Al; potassium carbonate / CH₂Cl₂ / 4 h / 0 - 20 °C

With sodium tetrahydroborate; N,N,N,N,-tetramethylethylenediamine; trimethylaluminum; sec.-butyllithium; tri-n-butyl-tin hydride; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; dichloromethane; cyclohexane; water; benzene; 6.2: Stille cross-coupling;
DOI:10.1016/j.tet.2007.05.127

Reference yield:

: 7524-52-9,26988-71-6,5619-09-0,14907-27-8,41222-70-2,67557-19-1,109492-62-8
(S)-tryptophan methyl ester hydrochloride

: 950886-76-7
C₃₈H₄₉IN₄O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylsilane; trifluoroacetic acid / 2 h / 50 °C

2.1: 33.4 g / Na₂CO₃ / dioxane; H₂O / 1.5 h / 20 °C

3.1: sodium borohydride; LiCl / tetrahydrofuran; ethanol / 5 h / 20 °C

4.1: 2.11 g / p-toluenesulfonic acid monohydrate / benzene / 3 h / 20 °C

5.1: s-BuLi; N,N,N',N'-tetramethylethylenediamine / diethyl ether; cyclohexane / 0.33 h / -78 °C

5.2: 73 percent / 1,2-diiodoethane / cyclohexane; diethyl ether / 0 - 20 °C

6.1: 47 percent / K₂CO₃; DDQ / benzene / 12 h / 70 °C

7.1: Bu₃SnH / Pd(PPh₃)4 / CH₂Cl₂ / -10 °C

7.2: copper(I) iodide; tri(2-furyl)phosphine / Pd₂(dba)3*CHCl₃ / 1-methyl-pyrrolidin-2-one

8.1: 82 percent / DMSO / 130 °C

9.1: 93 percent / Me₃Al; potassium carbonate / CH₂Cl₂ / 4 h / 0 - 20 °C

With triethylsilane; sodium tetrahydroborate; N,N,N,N,-tetramethylethylenediamine; trimethylaluminum; sec.-butyllithium; tri-n-butyl-tin hydride; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; dichloromethane; cyclohexane; water; benzene; 7.2: Stille cross-coupling;
DOI:10.1016/j.tet.2007.05.127