2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol

Base Information

Chemical Name:2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol
CAS No.:175519-63-8
Molecular Formula:C₂₃H₂₆N₂O₆
Molecular Weight:426.469
Hs Code.:

Synonyms:2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol

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Chemical Property of 2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol

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Technology Process of 2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol

There total 8 articles about 2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1356848-60-6
2-acetamido-4,6-O-benzylidene-1,5-(benzyloxycarbonyl)imino-3-O-tert-butyldimethylsilyl-1,2,5-trideoxy-D-glucitol

: 175519-63-8
2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ml2002746

Reference yield:

: C₂₁H₃₂N₂O₆Si

: 175519-63-8
2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfide borane / tetrahydrofuran; dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; dimethyl sulfide borane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ml2002746

Reference yield:

: C₂₁H₃₄N₂O₄Si

: 175519-63-8
2-acetamido-4,6-O-benzylidene-N-benzyloxycarbonyl-1,5-imino-1,2,5-trideoxy-D-glucitol

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ml2002746