p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside

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Chemical Name:p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside
CAS No.:1206803-27-1
Molecular Formula:C₄₀H₅₀O₅SSi
Molecular Weight:670.986
Hs Code.:

Synonyms:p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside

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Chemical Property of p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside

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Technology Process of p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside

There total 2 articles about p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 617-86-7
triethylsilane

: 211678-08-9
p-methylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

: 1206803-27-1
p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside

Guidance literature:: triethylsilane; With dicobalt octacarbonyl; carbon monoxide; at 20 ℃; for 0.25h; under 760.051 Torr;

p-methylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside; In benzene; at 50 ℃; for 18h; regioselective reaction;
DOI:10.1021/ol902717y

Reference yield:

: 617-86-7
triethylsilane

: 2,3,4-tri-O-Bn-6-O-Me-β-thiogalactoside

: 1206803-27-1
p-methylphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-galactopyranoside

Guidance literature:: triethylsilane; With dicobalt octacarbonyl; carbon monoxide; at 20 ℃; for 0.5h; under 760.051 Torr;

2,3,4-tri-O-Bn-6-O-Me-β-thiogalactoside; In toluene; at 70 ℃; for 48h; regioselective reaction;
DOI:10.1016/j.tet.2016.07.081