2,6-bis(dicyclohexylphosphinoxy)phenyliodopalladium

Base Information

• Chemical Name: 2,6-bis(dicyclohexylphosphinoxy)phenyliodopalladium
• CAS No.: 912651-64-0
• Molecular Formula: C₃₀H₄₇IO₂P₂Pd
• Molecular Weight: 734.974
• Mol file: 912651-64-0.mol

Synonyms:2,6-bis(dicyclohexylphosphinoxy)phenyliodopalladium

Chemical Property of 2,6-bis(dicyclohexylphosphinoxy)phenyliodopalladium

Chemical Property:

Purity/Quality:

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Technology Process of 2,6-bis(dicyclohexylphosphinoxy)phenyliodopalladium

There total 1 articles about 2,6-bis(dicyclohexylphosphinoxy)phenyliodopalladium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

trans-(2,6-dihydroxyphenyl)iodobis(triphenylphosphine)palladium*CH3CO2C2H5 + chlorodicyclohexylphosphane (16523-54-9) → 2,6-bis(dicyclohexylphosphinoxy)phenyliodopalladium (912651-64-0)

Guidance literature:

With Et₃N; In toluene; (N2); Et3N was added to suspn. of Pd complex in toluene at 0°C; Pcompd. (2.2 equiv.) was added at 0°C; mixt. was stirred at 25.de gree.C for 3 h; poured into H2O; extd. (CHCl3); org. layer dried (Na2SO4); filtered; concd. (vac.); chromd. (silica gel); elem. anal.;

DOI:10.1021/om060506b

upstream raw materials:

chlorodicyclohexylphosphane