allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate

Base Information

Chemical Name:allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate
CAS No.:329005-54-1
Molecular Formula:C₂₅H₃₅NO₆
Molecular Weight:445.556
Hs Code.:

Synonyms:allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate

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Chemical Property of allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate

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Technology Process of allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate

There total 6 articles about allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-{[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-amino}-6-(2-pent-4-enyl-[1,3]dioxolan-2-yl)-hexanoic acid allyl ester

: 329005-54-1
allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; for 1h;
DOI:10.1021/ol000361j

Reference yield:

: 106225-68-7
5-oxo-9-decenal

: 329005-54-1
allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 83 percent / CH₂Cl₂ / 1 h / 20 °C

2.1: 85 percent / HN₃; Et₃N / benzene / 27 h / Heating

3.1: 99 percent / trimethylsilyltriflate / CH₂Cl₂ / -78 - 20 °C

4.1: PPh₃ / tetrahydrofuran / 24 h / Heating

4.2: tetrahydrofuran / 32 h / Heating

5.1: 29 mg / 3-chloroperoxibenzoic acid / CH₂Cl₂ / 1 h / -78 - 20 °C

With tris-(2-chloro-ethyl)-amine; trimethylsilyl trifluoromethanesulfonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; benzene; 1.1: Wittig reaction / 4.1: Staudinger reaction / 4.2: aza-Wittig condensation;
DOI:10.1021/ol000361j

Reference yield:

: 104127-76-6
allyl (triphenylphosphoranylidene)acetate

: 329005-54-1
allyl 3-[3-(4-methoxyphenyl)oxaziridin-2-yl]-6-(2-pent-4-enyl[1,3]dioxolan-2-yl)hexanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 83 percent / CH₂Cl₂ / 1 h / 20 °C

2.1: 85 percent / HN₃; Et₃N / benzene / 27 h / Heating

3.1: 99 percent / trimethylsilyltriflate / CH₂Cl₂ / -78 - 20 °C

4.1: PPh₃ / tetrahydrofuran / 24 h / Heating

4.2: tetrahydrofuran / 32 h / Heating

5.1: 29 mg / 3-chloroperoxibenzoic acid / CH₂Cl₂ / 1 h / -78 - 20 °C

With tris-(2-chloro-ethyl)-amine; trimethylsilyl trifluoromethanesulfonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; benzene; 1.1: Wittig reaction / 4.1: Staudinger reaction / 4.2: aza-Wittig condensation;
DOI:10.1021/ol000361j