(1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(N(C₆H₄COOCH₃)CH(p-tolyl)2)

Base Information

• Chemical Name: (1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(N(C₆H₄COOCH₃)CH(p-tolyl)2)
• CAS No.: 676563-21-6
• Molecular Formula: C₅₄H₅₁N₂O₂P₂Rh
• Molecular Weight: 924.864

Synonyms:(1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(N(C₆H₄COOCH₃)CH(p-tolyl)2)

Chemical Property of (1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(N(C₆H₄COOCH₃)CH(p-tolyl)2)

Chemical Property:

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Technology Process of (1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(N(C₆H₄COOCH₃)CH(p-tolyl)2)

There total 1 articles about (1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(N(C₆H₄COOCH₃)CH(p-tolyl)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(p-tolyl) (676563-20-5) + 4-{[1-p-Tolyl-meth-(E)-ylidene]-amino}-benzoic acid methyl ester → (1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(N(C6H4COOCH3)CH(p-tolyl)2) (676563-21-6)

Guidance literature:

In toluene; (inert atm.); addn. of toluene to a mixt. of rhodium complex and ligand,stirring for 10-15 min at room temp.; concn., cooling to -35°C for 12 h, sepn. of ppt, washing with cold toluene, drying; elem. anal.;

DOI:10.1021/om0496582

upstream raw materials:

(1,2-bis(diphenylphosphino)ethane)Rh(pyridine)(p-tolyl)

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