methoxymethylphidolopin

Base Information

Chemical Name:methoxymethylphidolopin
CAS No.:99131-99-4
Molecular Formula:C₁₆H₁₇N₅O₆
Molecular Weight:375.341
Hs Code.:

Synonyms:methoxymethylphidolopin

Suppliers and Price of methoxymethylphidolopin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methoxymethylphidolopin

Chemical Property:

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Technology Process of methoxymethylphidolopin

There total 3 articles about methoxymethylphidolopin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 58-55-9,75448-53-2
theophylline

: 99132-02-2
4-(methoxymethoxy)-3-nitrobenzyl bromide

: 99131-99-4
methoxymethylphidolopin

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4039(00)95097-4

Reference yield:

: 119-33-5
4-methyl-2-nitrophenol

: 99131-99-4
methoxymethylphidolopin

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / NaH / tetrahydrofuran / Ambient temperature

2: N-bromosuccinimide / α,α'-azobis-iso-butyronitrile / CCl4

3: 99 percent / K₂CO₃ / dimethylformamide / Ambient temperature

With N-Bromosuccinimide; sodium hydride; potassium carbonate; azobisisobutyronitrile; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)95097-4

Reference yield:

: 99132-01-1
1-methoxymethoxy-4-methyl-2-nitrobenzene

: 99131-99-4
methoxymethylphidolopin

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide / α,α'-azobis-iso-butyronitrile / CCl4

2: 99 percent / K₂CO₃ / dimethylformamide / Ambient temperature

With N-Bromosuccinimide; potassium carbonate; azobisisobutyronitrile; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)95097-4