9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

Base Information

Chemical Name:9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene
CAS No.:1283598-74-2
Molecular Formula:C₃₉H₂₅BrN₂
Molecular Weight:601.545
Hs Code.:

Synonyms:9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

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Chemical Property of 9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

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Technology Process of 9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

There total 4 articles about 9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1283598-73-1
9-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

: 1283598-74-2
9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

Guidance literature:: With N-Bromosuccinimide; In chloroform; at 50 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c0jm03300f

Reference yield:

: 1564-64-3
9-Bromoanthracene

: 1283598-74-2
9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / 12 h / Reflux; Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / 12 h / Reflux; Inert atmosphere

4.1: N-Bromosuccinimide / chloroform / 2 h / 50 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; chloroform; 2.1: Suzuki coupling / 3.1: Suzuki coupling;
DOI:10.1039/c0jm03300f

Reference yield:

: 100622-34-2
anthracene-9-boronic acid

: 1283598-74-2
9-bromo-10-[4-(1-phenyl-1H-benzimidazol-2-yl)-biphenyl-4'-yl]anthracene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / 12 h / Reflux; Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / 12 h / Reflux; Inert atmosphere

3: N-Bromosuccinimide / chloroform / 2 h / 50 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; chloroform; 1: Suzuki coupling / 2: Suzuki coupling;
DOI:10.1039/c0jm03300f