C₃₀H₄₈O₈

Base Information

Chemical Name:C₃₀H₄₈O₈
CAS No.:1313484-47-7
Molecular Formula:C₃₀H₄₈O₈
Molecular Weight:536.706
Hs Code.:

C<sub>30</sub>H<sub>48</sub>O<sub>8</sub>

Synonyms:C₃₀H₄₈O₈

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Chemical Property of C₃₀H₄₈O₈

Chemical Property:

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Technology Process of C₃₀H₄₈O₈

There total 16 articles about C₃₀H₄₈O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1313484-46-6
C₃₀H₄₈O₈

: 1313484-47-7
C₃₀H₄₈O₈

Guidance literature:: C₃₀H₄₈O₈; With potassium hexamethylsilazane; In toluene; at -78 ℃; for 2h; Inert atmosphere;

With chloro-trimethyl-silane; In toluene; at -78 - 85 ℃; for 20.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c1cc11388g

Reference yield:

: 928618-22-8
(2'S,3'S,4R,5R)-2-hydroxymethyl-4-O,5-O-(2',3'-dimethoxybutane-2',3'-diyl)-4,5-dihydroxycyclohex-2-en-1-one

: 1313484-47-7
C₃₀H₄₈O₈

Guidance literature:: Multi-step reaction with 9 steps

1.1: dmap; triethylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

2.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 0 °C / Inert atmosphere

3.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h / 0 °C / Inert atmosphere

4.1: triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid / toluene / 15 h / 20 °C / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane; water / 0.17 h / 20 °C / Inert atmosphere

6.1: pyridine; dmap / 48 h / 20 °C / Inert atmosphere

7.1: pyridine hydrogenfluoride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

8.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 19 h / 20 °C / Inert atmosphere

9.1: potassium hexamethylsilazane / toluene / 2 h / -78 °C / Inert atmosphere

9.2: 20.5 h / -78 - 85 °C / Inert atmosphere

With pyridine; dmap; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium tetrahydroborate; cerium(III) chloride heptahydrate; potassium hexamethylsilazane; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; lithium hexamethyldisilazane; diethylazodicarboxylate; 4-nitro-benzoic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 3.1: Luche reduction / 4.2: Mitsunobu reaction / 9.1: Ireland-Claisen rearrangement / 9.2: Ireland-Claisen rearrangement;
DOI:10.1039/c1cc11388g

Reference yield:

: 1313484-43-3
C₂₉H₃₈O₆Si

: 1313484-47-7
C₃₀H₄₈O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 0 °C / Inert atmosphere

2.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h / 0 °C / Inert atmosphere

3.1: triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid / toluene / 15 h / 20 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane; water / 0.17 h / 20 °C / Inert atmosphere

5.1: pyridine; dmap / 48 h / 20 °C / Inert atmosphere

6.1: pyridine hydrogenfluoride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

7.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 19 h / 20 °C / Inert atmosphere

8.1: potassium hexamethylsilazane / toluene / 2 h / -78 °C / Inert atmosphere

8.2: 20.5 h / -78 - 85 °C / Inert atmosphere

With pyridine; dmap; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium tetrahydroborate; cerium(III) chloride heptahydrate; potassium hexamethylsilazane; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; trifluoroacetic acid; lithium hexamethyldisilazane; diethylazodicarboxylate; 4-nitro-benzoic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 2.1: Luche reduction / 3.2: Mitsunobu reaction / 8.1: Ireland-Claisen rearrangement / 8.2: Ireland-Claisen rearrangement;
DOI:10.1039/c1cc11388g