3-CHLORO-2,6-DIMETHOXYBENZOIC ACID, 97

Base Information

• Chemical Name: 3-CHLORO-2,6-DIMETHOXYBENZOIC ACID, 97
• CAS No.: 36335-47-4
• Molecular Formula: C9H9 Cl O4
• Molecular Weight: 216.621
• Hs Code.: 2918990090
• Mol file: 36335-47-4.mol

Synonyms:3-Chloro-2,6-dimethoxybenzoicacid; 5-Chloro-2,6-dimethoxybenzoic acid

Chemical Property of 3-CHLORO-2,6-DIMETHOXYBENZOIC ACID, 97

Chemical Property:

• Melting Point: 131-133°C
• PSA: 55.76000
• LogP: 2.05540

Purity/Quality:

98%Min ^*data from raw suppliers

3-Chloro-2,6-dimethoxybenzoic acid ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-CHLORO-2,6-DIMETHOXYBENZOIC ACID, 97

There total 3 articles about 3-CHLORO-2,6-DIMETHOXYBENZOIC ACID, 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-6-dimethoxybenzoic acid (1466-76-8) → 2,6-dimethoxy-3-chlorobenzoic acid (36335-47-4)

Guidance literature:

With N-chloro-succinimide; 2,2,6,6-tetramethylpiperidin-1-oxoammonium trifluoromethanesulfonate; In chloroform; at 25 ℃; for 12h; Reagent/catalyst; Schlenk technique;

Reference yield:

2,6-dimethoxyacetophenone (2040-04-2) → 2,6-dimethoxy-3-chlorobenzoic acid (36335-47-4)

Guidance literature:

With sodium hypochlorite;

Reference yield:

→ 2,6-dimethoxy-3-chlorobenzoic acid (36335-47-4)

Guidance literature:

aus Benzoesaeure 2a mit Sulfurylchlorid;

upstream raw materials:

2,6-dimethoxyacetophenone

2-6-dimethoxybenzoic acid

Downstream raw materials:

3-chloro-2,6-dimethoxybenzoyl chloride

3-bromo-5-chloro-2,6-dimethoxybenzoic acid

A 32507 hydrochloride

N-[1-acetyl-5,7-dimethoxy-4-(4-methoxyphenyl)-2,2,4-trimethyl-1,2,3,4-tetrahydroquinolin-6-yl]-3-chloro-2,6-dimethoxybenzamide